Synthesis of 9,10-diacetoxyanthracene

Preparation of 9,10-diacetoxyanthracene

One part of anthraquinone is boiled for a short time with 10 to 15 parts of acetic anhydride, 2, parts of anhydrous sodium acetate, and 3 parts of zinc dust. The solution after cooling is filtered, the residue dissolved in a little boiling glacial acetic acid, filtered hot, and the filtrate allowed to cool. The 9,10-diacetoxyanthracene is collected, and recrystallised several times from glacial acetic acid. It forms colourless needles which melt at 260° C.

Preparation of organic compounds, E. de. Barry Barnett, 94, 1912

IUPAC Name

(10-acetyloxyanthracen-9-yl) acetate

InChI

InChI=1S/C18H14O4/c1-11(19)21-17-13-7-3-5-9-15(13)18(22-12(2)20)16-10-6-4-8-14(16)17/h3-10H,1-2H3

InChI Key

RURGWVZQAKAYDM-UHFFFAOYSA-N

Canonical SMILES

CC(=O)OC1=C2C=CC=CC2=C(C3=CC=CC=C31)OC(=O)C

Depositor-Supplied Synonyms

9,10-Diacetoxyanthracene, 9,10-Anthracenediol, diacetate, Anthrahydroquinone diacetate, 9,10-Anthradiol, diacetate, anthracene-9,10-diyl diacetate, 604-66-0, 1,10-Dihydroxyanthracene diacetate, STK398375, BRN 2335936, AC1L3T0I, Oprea1_423860, CBDivE_002933, AC1Q620Q, SCHEMBL6907648, CHEBI:51306, CTK2F5414, NSC4719, MolPort-002-110-775, RURGWVZQAKAYDM-UHFFFAOYSA-N, NSC-4719, ZINC2810011, Diaceticacid9,10-anthracenediylester, AR-1H5158, ZINC02810011, (10-acetyloxyanthracen-9-yl) acetate, 10-(Acetyloxy)-9-anthryl acetate #, AKOS004907189, MCULE-2820170329, LS-20298, PL061424, 10-(ACETYLOXY)ANTHRACEN-9-YL ACETATE, AB01334841-02, 4-06-00-06892 (Beilstein Handbook Reference)

Removed Synonyms

CID94838, 62203-32-1

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