Synthesis of bis(4-bromobenzoyl) peroxide

Preparation of bis(4-bromobenzoyl) peroxide A solution of 8.5 g. (0.04 mole) of 4-bromobenzoyl ... Read more

Synthesis of 4-bromobenzoyl chloride

Preparation of 4-bromobenzoyl chloride A mixture of 35 g. (0.17 mole) of p-bromobenzoic acid ... Read more

Preparation of 3-(4-bromophenyl)-1-propene A solution of 130 g. (1.08 moles) of allyl bromide ... Read more

Preparation of boron trifluoride dihydrate One mole (67.8 g.) of boron trifluoride is absorbed ... Read more

Preparation of bis(2-aminoethyl)sulfide Forty-three grams (1.0 mole) of ethyleneimine is placed ... Read more

Preparation of phenyl sodium A mixture of 150 ml. of toluene, 11.5 g. (0.5 gram atom) of sodium ... Read more

Preparation of benzyl phenyl sulfide Thiophenol (57 g., 0.52 mole) is added slowly with ... Read more

Preparation of benzoyl azide A solution of 37 g. (0.57 mole) of sodium azide in 100 ml. of ... Read more

Preparation of benzal diacetate Ten grams (0.094 mole) of benzaldehyde (free of benzoic acid) ... Read more

Preparation of m-anisidine A mixture of 35 g. (0.23 mole) of m-nitroanisole (p. 213), 110 ml. ... Read more

Preparation of Caro’s acid (Peroxymonosulfuric acid) A slight excess of 100% (or at least ... Read more

Preparation of deuterium Flask E of the glass apparatus shown in figure contains an Al crucible ... Read more

Preperation of hydrogen peroxide Hydrogen peroxide is conveniently prepared by slowly adding 10 ... Read more

Preparation of diazobenzene nitrate (benzenediazonium nitrate) Owing to the highly explosive ... Read more

Preparation of phenylhydrazine 10 g. freshly distilled aniline are added to a solution of 30 g. ... Read more