Synthesis of N-acetylethylenediamine

Preparation of N-acetylethylenediamine

Preparation of N-acetylethylenediamine

Preparation of N-acetylethylenediamine

A mixture of 528 g. (6.0 moles) of ethyl acetate and 1550 g. (18.0 moles) of a 70% aqueous solution of ethylenediamine is allowed to stand for several days after it has become homogeneous. The material is distilled, and the fraction boiling in the range 115-130°/5 mm. is redistilled to give 365 g. (60%) of the monoacetyl derivative, b.p. 125-130°/5 mm. The product contains traces of ethylenediamine, lysidine, and diacetylethylenediamine.

J. Am. Chem. Soc., 63, 853, 1941

IUPAC Name

N-(2-aminoethyl)acetamide

InChI

InChI=1S/C4H10N2O/c1-4(7)6-3-2-5/h2-3,5H2,1H3,(H,6,7)

InChI Key

DAKZISABEDGGSV-UHFFFAOYSA-N

Canonical SMILES

CC(=O)NCCN

MeSH Synonyms

N-(2-aminoethyl)acetamide

Depositor-Supplied Synonyms

N-Acetylethylenediamine, N-(2-Aminoethyl)acetamide, 1001-53-2, N-(2-Amino-ethyl)-acetamide, Acetamide, N-(2-aminoethyl)-, DAKZISABEDGGSV-UHFFFAOYSA-N, acetylethylenediamine, NSC28936, 2-acetamidoethylamine, acetylethylene diamine, N-acetylethylendiamine, 2-acetylaminoethylamine, monoacetylethylenediamine, PubChem19141, N-acetyl-ethylenediamine, N-acetylethylene diamine, N-acetylethylene-diamine, 2-acetylamino-ethylamine, monoacetyl-ethylenediamine, N-(acetyl)ethylenediamine, UNII-FQL33V3KZD, FQL33V3KZD, N-Monoacetylethylenediamine, (2-acetylaminoethyl)-amine, 2-(acetylamino)-ethylamine, AC1Q1L6P, N-(2-aminoethyl) acetamide, N-(2-aminoethyl)-acetamide, N-acetylethane-1,2-diamine, SCHEMBL43340, mono-N-acetylethylene diamine, KSC492S3R, N-(2-Aminoethyl)acetamide #, ACMC-2097n0, 397261_ALDRICH, AC1L24L2, Acetamide, N-(2-aminoethyl-), CTK3J2938, DAKZISABEDGGSV-UHFFFAOYSA-, MolPort-001-791-776, BB_SC-8012, ACN-S003828, ACT06646, ANW-14170, BBL027688, NSC 28936, NSC-28936, SBB028176, STL259802, AKOS000121496, AC-7474, AN-8959, MCULE-2230084818, AJ-28799, AK-81466, KB-55328, SC-19651, AB0019923, RT-001126, ST2419644, A0887, UX00000418, V0519, Acetamide, N-(2-aminoethyl)- (8CI)(9CI), A16155, K-0149, 132982-EP2287155A1, 132982-EP2295438A1, I05-0152, T5429089, 3B3-030490, InChI=1/C4H10N2O/c1-4(7)6-3-2-5/h2-3,5H2,1H3,(H,6,7)

Removed Synonyms

CID66082

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