Synthesis of dinitrosopentamethylenetetramine

Preparation of dinitrosopentamethylenetetramine

Alternative Names: 3,7-dinitroso-1,3,5,7-tetrazabicyclo[3.3.1]nonane; N,N’-Dinitrosopentamethylenetetramine; Dipentax; Micropor; Dnpmt; Opex; Mikrofor N; Porophor B; Di-N-nitrosopentamethylenetetramine;

Preparation of dinitrosopentamethylenetetramine

Preparation of dinitrosopentamethylenetetramine

To an ice-cold solution of 7 g of hexamethylenetetramine and 9.7 ml of acetic acid in 450 ml of water was added an ice-cold solution of 10.4 g of sodium nitrite dissolved in 50 ml of water. Dinitrosopentamethylenetetramine was collected by filtration after one hour, washed with small amount of cold water. The yield is 5 g, m.p. 206-209° C.

J. Am. Chem. Soc., 1951, 73 (6), pp 2777–2779

IUPAC Name

3,7-dinitroso-1,3,5,7-tetrazabicyclo[3.3.1]nonane

InChI

InChI=1S/C5H10N6O2/c12-6-10-2-8-1-9(4-10)5-11(3-8)7-13/h1-5H2

InChI Key

MWRWFPQBGSZWNV-UHFFFAOYSA-N

Canonical SMILES

C1N2CN(CN1CN(C2)N=O)N=O

MeSH Synonyms

dinitrosopentamethylenetetramine

Depositor-Supplied Synonyms

Dipentax, Micropor, Dnpmt, Opex, Mikrofor N, Porophor B, Vulcacel BN, Unicel-ND, Aceto DNPT 100, Unicel NDX, 101-25-7, Porofor DNO/F, Porofor chkhc-18, Vulcacel B-40, DNMPT, DNPT, Khempor N 90, Aceto DNPT 40, Aceto DNPT 80, ChKhz 18, Opex 93, Dinitrosopentamethenetetramine, N,N-Dinitrosopentamethylenetetramine, N,N’-Dinitrosopentamethylenetetramine, Dinitrosopentamethylenetetraamine, 3,7-Dinitroso-1,3,5,7-tetraazabicyclo[3.3.1]nonane, Di-N-nitrosopentamethylenetetramine, Pentamethylenetetramine, dinitroso-, Unicel ND, Vulcacel BN 94, Cellmic A 80, Chempor N 90, Chempor PC 65, Porofor ChKhZ-18, Unicel 100, NSC 73599, CHKHZ-18, 3,7-Di-N-nitrosopentamethylenetetramine, 3,7-Dinitroso-1,3,5,7-tetraazabicyclo(3.3.1)nonane, 1,3,5,7-Tetraazabicyclo[3.3.1]nonane, 3,7-dinitroso-, NSC73599, N(sup 1),N(sup 3)-dinitrosopentamethylenetetramine, 3,7-dinitroso-1,3,5,7-tetrazabicyclo[3.3.1]nonane, N(Sup1),N(Sup3)-Dinitrosopentamethylenetetramine, 1,5-Methylene-3,7-dinitroso-1,3,5,7-tetraazacyclooctane, 85605-18-1, 1,3,5,7-Tetraazabicyclo(3.3.1)nonane, 3,7-dinitroso-, UNII-O35M5QNM4Q, AC1L1P0J, AC1Q6RA9, O35M5QNM4Q, SCHEMBL138395, CHEBI:82457, CTK5F5323, MolPort-006-110-520, MWRWFPQBGSZWNV-UHFFFAOYSA-N, AR-1F0225, N, N-Dinitrosopentamethylenetetramine, NSC-73599, AKOS006230411, N, N’-Dinitrosopentamethylenetetramine, N1,N3-Dinitrosopentamethylenetetramine, 3, 7-Di-N-nitrosopentamethylenetetramine, 3,3,5,7-tetraazabicyclo(3,3,1)nonane, AJ-72839, AK139989, AN-24571, PL003172, RT-000240, WLN: T66 A BN DN FN HNTJ DNO HNO, 1,7-dinitroso-1,3,5,7-tetraazacyclooctane, D0851, C19409, 5-26-11-00042 (Beilstein Handbook Reference), N(sup1), N(sup3)-Dinitrosopentamethylenetetramine, N,N’-DINITROSOPENTA-METHYLENETETRAMINE, PURE, I14-46688, 1,3,5,7-Tetraazabicyclo[3.3.1]nonane,3,7-dinitroso-, 1,5,7-Tetraazabicyclo[3.3.1]nonane, 3,7-dinitroso-, 3,7-Dinitroso-1,3,5, 7-tetraazabicyclo(3,3,1)nonane, 3B1-000066, 1, 5-Methylene-3,7-dinitroso-1,3,5,7-tetraazacyclooctane, 3,7-Dinitroso-1,3,5, {7-tetraazabicyclo[3.3.1]nonane}, 1,3,5, {7-Tetraazabicyclo[3.3.1]nonane,} 3,7-dinitroso-, 1,5-endo-Methylene-3,7-dinitroso-1,3,5,7-tetraazacyclooctane, 1, 5-endo-Methylene-3,7-dinitroso-1,3,5,7-tetraazacyclooctane, 42617-17-4, 42617-18-5, 50337-90-1, 52229-98-8

Removed Synonyms

Celmike A, Porotor DNO/F, Diasalt Bordeaux GP, Opex 80, DINITROSOPENTAMETHYLENETETRAMINE, CCRIS 8924, Dinitrosopentamethylene tetramine, HSDB 4309, CID7549, EINECS 202-928-3, 3,4-Di-N-nitrosopentamethylenetetramine, BRN 0180027, 3,3,5,7-tetraazabicyclo[3.3.1]nonane, AI3-52486, N(1),N(3)-Dinitrosopentamethylenetetramine, 3,7-Dinitroso-1,3,5,7-tetraazabicyclo-(3,3,1)-nonane, 1,5-Endomethylene-3,7-dinitroso-1,3,5,7-tetraazacyclooctane, 92100-11-3

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