Synthesis of acetone phenylhydrazone

Preparation of acetone phenylhydrazone

Preparation of acetone phenylhydrazone

Preparation of acetone phenylhydrazone

10 ml of glacial acetic acid is mixed with 10.8 g of phenylhydrazine. The solution is diluted with 10 ml of water, and 5.8 g of acetone are added. The acetone phenylhydrazone which separates is extracted with ether. The latter is separated, dried over aydrous potassium carbonate, and distilled under reduced pressure, the fraction 165° C/91 mm. being retaned. The obtained acetone phenylhydrazone is allowed to stand in a vacuum desiccator over sulphutic acid for a short time. Yied almost theoretical, colorless, somewhat unstable oil b.p. 165° C/91 mm.

Systematic organic chemistry, by W. M. Cumming, 290, 1937.

IUPAC Name

N-(propan-2-ylideneamino)aniline

InChI

InChI=1S/C9H12N2/c1-8(2)10-11-9-6-4-3-5-7-9/h3-7,11H,1-2H3

InChI Key

JQLKSEQEILIJEG-UHFFFAOYSA-N

Canonical SMILES

CC(=NNC1=CC=CC=C1)C

MeSH Synonyms

acetone phenylhydrazone

Depositor-Supplied Synonyms

Acetone phenylhydrazone, 103-02-6, 2-Propanone, phenylhydrazone, 1-Phenyl-2-(propan-2-ylidene)hydrazine, 2-Propanone, 2-phenylhydrazone, JQLKSEQEILIJEG-UHFFFAOYSA-N, PubChem19806, Acetone phenyl hydrazone, Acetone, phenylhydrazone, AC1L24GH, 2-Propanone,2-phenylhydrazone, SCHEMBL3086579, CTK4A1671, N-(propan-2-ylideneamino)aniline, MolPort-006-110-566, N-Isopropylidene-N’-phenylhydrazine, NSC65251, ZINC4758208, EINECS 203-071-8, 8097AF, NSC 65251, NSC-65251, AKOS006230254, MCULE-5590733746, AJ-52167, AK136957, EN001652, OR039891, OR195323, AI3-15277, KB-219636, InChI=1/C9H12N2/c1-8(2)10-11-9-6-4-3-5-7-9/h3-7,11H,1-2H

Removed Synonyms

CID66026, C045543, 80466-56-4

Share This

Leave a Reply

Your email address will not be published. Required fields are marked *