Synthesis of 2-naphthyl acetate

Preparation of 2-naphthyl acetate

Preparation of 2-naphthyl acetate

Preparation of 2-naphthyl acetate

To 1 gram of pure 2-naphthol in 5 ml  of 10 % sodium hydroxide solution, 10 grams of crushed ice and 1.1 ml  of acetic anhydride are added. The mixture is vigorously mixed for about 10-15 minutes. The 2-naphthyl acetate separates as colorless crystals which are filtered and wash with water. Yield of crude material is about 1.4 grams. Recrystallization from petroleum, from which, on cooling the 2-naphthyl acetate separates as colorless crystals, yield 1 gram of final product with melting point 71° C.

Practical organic chemistry, 1960, 110.

IUPAC Name

naphthalen-2-yl acetate

InChI

InChI=1S/C12H10O2/c1-9(13)14-12-7-6-10-4-2-3-5-11(10)8-12/h2-8H,1H3

InChI Key

RJNPPEUAJCEUPV-UHFFFAOYSA-N

Canonical SMILES

CC(=O)OC1=CC2=CC=CC=C2C=C1

Depositor-Supplied Synonyms

2-Naphthyl acetate, 1523-11-1, naphthalen-2-yl acetate, 2-Naphthalenol, acetate, 2-Acetoxynaphthalene, 2-Naphthol, acetate, beta-Naphthyl acetate, Naphthalene, 2-acetoxy-, 2-Naphthalenol, 2-acetate, .beta.-Naphthol acetate, .beta.-Naphthyl acetate, O-Acetyl-.beta.-naphthol, RJNPPEUAJCEUPV-UHFFFAOYSA-N, NSC 37069, ST50825247, beta-Naphthol acetate, O-Acetyl-beta-naphthol, AC1L2KCA, ACMC-209d7n, KSC489Q7N, 2-Naphthol, acetate (8CI), Acetic Acid 2-Naphthyl Ester, N6875_SIGMA, SCHEMBL338523, AC1Q627B, CTK3I9876, MolPort-000-564-590, Acetic acid .beta.-naphthyl ester, NSC37069, EINECS 216-194-7, ANW-21393, AR-1E4287, NSC-37069, ZINC00388670, AKOS015899138, MCULE-4875836262, RP24624, RTR-030951, VZ25033, AJ-20724, AK105947, AN-49379, CJ-03320, KB-69408, ZB011646, AI3-17247, TR-030951, A0038, FT-0613139, ST24048778, I14-1270, 3B3-013521, InChI=1/C12H10O2/c1-9(13)14-12-7-6-10-4-2-3-5-11(10)8-12/h2-8H,1H

Removed Synonyms

OOEa-|A-YAo yen, 2-NAPHTHYLACETATE, CID73709, 15482-38-9

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