Synthesis of 4-chlorobutyl acetate

Preparation of 4-chlorobutyl acetate

Preparation of 4-chlorobutyl acetate

Preparation of 4-chlorobutyl acetate

Acetyl chloride (65 g), tetrahydrofuran (50 g; b.p. 66°), and zinc chloride (0.01 g) are boiled for 90 min under reflux with exclusion of moisture, whereafter distillation gives 76% of 4-chlorobutyl acetate, b.p. 78-79°/15 mm, 90-91°/20 mm.

J. Amer. Chem. Soc, 61, 2667 (1939).


4-chlorobutyl acetate



InChI Key


Canonical SMILES


Depositor-Supplied Synonyms

4-Chlorobutyl acetate, 6962-92-1, 1-Acetoxy-4-chlorobutane, 4-Chloro-n-butyl acetate, 1-Chloro-4-acetoxybutane, 1-BUTANOL, 4-CHLORO-, ACETATE, 4-Chloro-1-butanol acetate, 4-Chlorbut-1-ylacetat, delta-Chlorobutyl acetate, 1-Butanol, 4-chloro-, 1-acetate, NSC 53492, NSC 54074, Acetic Acid 4-Chlorobutyl Ester, 4-Chlorbut-1-ylacetat [German], PYLDCZJUHYVOAF-UHFFFAOYSA-N, EINECS 230-158-8, SBB059334, BRN 1749681, AI3-16503, .omega.-Chlorobutyl acetate, PubChem13100, AC1Q1LCL, ACMC-1B6NR, .delta.-Chlorobutyl acetate, AC1L2M9M, C29207_ALDRICH, KSC493G2F, SCHEMBL1270067, Acetic acid=4-chlorobutyl ester, CTK3J3322, PYLDCZJUHYVOAF-UHFFFAOYSA-, acetic acid 4-chloro-butyl ester, NSC53492, NSC54074, ZINC1684560, ANW-35728, MFCD00001013, NSC-53492, NSC-54074, ZINC01684560, AKOS006221691, MCULE-3999602136, TRA0031588, AJ-29799, AK110810, CJ-06360, LS-46464, OR040241, U210, KB-151698, FT-0607276, ST51040041, AZ0001-0270, EN300-66013, A-7489, 4-02-00-00147 (Beilstein Handbook Reference), W-104612, I14-50528, 3B1-007434, F0001-1810, InChI=1/C6H11ClO2/c1-6(8)9-5-3-2-4-7/h2-5H2,1H3

Removed Synonyms

4-chlorobutylacetate, 1-Butanol, acetate, C6H11ClO2, MolPort-001-791-986, CID23399, RT-001410, A1098

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