Synthesis of 4-bromo-N,N-dimethylaniline

Preparation of 4-bromo-N,N-dimethylaniline

Preparation of 4-bromo-N,N-dimethylaniline

Preparation of 4-bromo-N,N-dimethylaniline

10 g. dimethylaniline are dissolved in glacial acetic acid, and 6.6 g. bromine dissolved in glacial acetic acid gradually added. When the solution is diluted with water, the 4-bromo-N,N-dimethylaniline is precipitated, filtered off, and recrystallised from alcohol. The yield almost theoretical (16–17 g). White plates; M.P. 55 °C.

Systematic organic chemistry, by W. M. Cumming, 353, 1937.

IUPAC Name

4-bromo-N,N-dimethylaniline

InChI

InChI=1S/C8H10BrN/c1-10(2)8-5-3-7(9)4-6-8/h3-6H,1-2H3

InChI Key

XYZWMVYYUIMRIZ-UHFFFAOYSA-N

Canonical SMILES

CN(C)C1=CC=C(C=C1)Br

Depositor-Supplied Synonyms

4-Bromo-N,N-dimethylaniline, 586-77-6, N,N-Dimethyl-p-bromoaniline, p-Bromo-N,N-dimethylaniline, 4-Dimethylaminobromobenzene, N,N-Dimethyl-4-bromoaniline, Benzenamine, 4-bromo-N,N-dimethyl-, p-(Dimethylamino)phenyl bromide, p-Dimethylaminobromobenzene, 1-Bromo-4-(dimethylamino)benzene, p-Bromo(dimethylamino)benzene, p-N,N-Dimethylaminobromobenzene, N-(4-bromophenyl)-N,N-dimethylamine, ANILINE, 4-BROMO-N,N-DIMETHYL-, 4-(Dimethylamino)phenyl bromide, Aniline, p-bromo-N,N-dimethyl-, NSC 8056, (4-bromophenyl)dimethylamine, 4-bromo-n,n-dimethyl aniline, 4-bromo-N,N-dimethyl-aniline, 4-Bromo-N,N-dimethylbenzenamine, XYZWMVYYUIMRIZ-UHFFFAOYSA-N, EINECS 209-582-2, MFCD00000093, AC-509/25001966, PubChem2230, AC1L1XEV, AC1Q3WKQ, ACMC-209m6e, 4-dimethylaminophenyl bromide, SCHEMBL59844, p-bromo-n,n-dimethyl aniline, KSC270S7J, WLN: ER DN1&1, 4-dimethylamino-1-bromobenzene, 242950_ALDRICH, AC1Q3W76, AC1Q3W77, CHEMBL3098160, DTXSID2060414, (4-bromo-phenyl)-dimethyl-amine, 16920_FLUKA, CTK1H0974, 4-bromo-n,n-dimethyl-benzenamine, NSC8056, ZINC330697, NSC-8056, AN-311, ANW-33012, LABOTEST-BB LT02084978, LABOTEST-BB LT03329517, LABOTEST-BB LT03496170, SBB058575, ZINC00330697, AKOS005256709, CS15132, LS10693, MCULE-2796271299, RP25755, RP25756, TRA0089789, Aniline, p-bromo-N,N-dimethyl- (8CI), AJ-19326, AK-47628, BC002256, BR-47628, CJ-02740, H253, KB-37411, LS-19611, OR011479, SC-05545, ZB010505, DB-053244, TR-020384, A8294, AM20060845, B0585, FT-0617904, ST24032767, ST50405356, EN300-19549, M-5960, I01-0565, W-105368, F9995-1667, InChI=1/C8H10BrN/c1-10(2)8-5-3-7(9)4-6-8/h3-6H,1-2H, 508191-89-7

Removed Synonyms

Aniline,N-dimethyl-, Benzenamine,N-dimethyl-, C8H10BrN, MolPort-000-151-961, CID11465, RTR-020384

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