Synthesis of 2-amino-2-thiazoline Preparation of 2-amino-2-thiazoline 100 g of potassium thiocyanate are added to a solution of ... Read more
Synthesis of 3-chlorobenzaldehyde Preparation of 3-chlorobenzaldehyde 2 moles of tin(II) chloride dihydrate are dissolved in ... Read more
Synthesis of dichloromethyl methyl ether Preparation of dichloromethyl methyl ether 832 g (4.0 moles) of phosphorus pentachloride and ... Read more
Synthesis of 1,2-phenylene phosphorotrichloridite Preparation of 1,2-phenylene phosphorotrichloridite Chlorine is passed into a stirred ... Read more
Synthesis of oxalyl bromide Preparation of oxalyl bromide Oxalyl bromide is obtained by passing hydrogen bromide (8 ... Read more
Synthesis of heptanenitrile Preparation of heptanenitrile 30 g of dry sodium cyanide (dried at 110º C overnight a) are ... Read more
Synthesis of allyl alcohol-1,1-d2 Preparation of allyl alcohol-1,1-d2 6 g of lithium aluminum deuteride are made into a slurry ... Read more
Synthesis of benzyl p-toluenesulfonate Preparation of benzyl p-toluenesulfonate 22g of tosyl chloride were dissolved in 88 ml of dry ... Read more
Synthesis of 4-chlorobutyl acetate Preparation of 4-chlorobutyl acetate Acetyl chloride (65 g), tetrahydrofuran (50 g; b.p. 66°), ... Read more
Synthesis of 3-amino-2,4,6-triiodobenzoic acid Preparation of 3-amino-2,4,6-triiodobenzoic acid A mixture containing 290 g of iodine chloride ... Read more
Synthesis of sodium dichloroiodate Preparation of sodium dichloroiodate Sodium dichloroiodate is prepared as 2M-soIution. 520g of ... Read more
Synthesis of capronitrile Preparation of capronitrile 30 g of dry sodium cyanide (dried at 110º C overnight a) are mixed ... Read more
Synthesis of n-butane-1-d Preparation of n-butane-1-d 11 g of deuterium oxide are added slowly to a vigorously stirred ... Read more
Synthesis of picryl chloride Preparation of picryl chloride Pyridine (7.9) is added to a hot solution of picric acid (22.9 ... Read more
Synthesis of 4-chloro-1-butanol Preparation of 4-chloro-1-butanol 4-Chloro-1-butanol is obtained simply by leading hydrogen ... Read more