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Synthesis of 2-amino-2-thiazoline

Synthesis of 2-amino-2-thiazoline
Preparation of 2-amino-2-thiazoline 100 g of potassium thiocyanate are added to a solution of ... Read more
Aug 23
1026 0 Amines, Five-membered heterocycles, Heterocycles, Organics www.PrepChem.com

Synthesis of 3-chlorobenzaldehyde

Synthesis of 3-chlorobenzaldehyde
Preparation of 3-chlorobenzaldehyde 2 moles of tin(II) chloride dihydrate are dissolved in ... Read more
Aug 22
1243 0 Aldehydes, Halocarbons, Organics, Organochlorine Compounds www.PrepChem.com

Synthesis of dichloromethyl methyl ether

Synthesis of dichloromethyl methyl ether
Preparation of dichloromethyl methyl ether 832 g (4.0 moles) of phosphorus pentachloride and ... Read more
Aug 22
1024 0 Ethers, Halocarbons, Organics, Organochlorine Compounds www.PrepChem.com

Synthesis of 1,2-phenylene phosphorotrichloridite

Synthesis of 1,2-phenylene phosphorotrichloridite
Preparation of 1,2-phenylene phosphorotrichloridite Chlorine is passed into a stirred ... Read more
Aug 22
549 0 Halocarbons, Organics, Organochlorine Compounds, Organophosphorus compounds www.PrepChem.com

Synthesis of oxalyl bromide

Synthesis of oxalyl bromide
Preparation of oxalyl bromide Oxalyl bromide is obtained by passing hydrogen bromide (8 ... Read more
Aug 22
1279 0 Halocarbons, Organics, Organobromine Compound www.PrepChem.com
Synthesis submission

Synthesis of heptanenitrile

Synthesis of heptanenitrile
Preparation of heptanenitrile 30 g of dry sodium cyanide (dried at 110º C overnight a) are ... Read more
Aug 22
719 0 Nitriles, Organics www.PrepChem.com

Synthesis of allyl alcohol-1,1-d2

Synthesis of allyl alcohol-1,1-d2
Preparation of allyl alcohol-1,1-d2 6 g of lithium aluminum deuteride are made into a slurry ... Read more
Aug 22
656 0 Alcohols, Deuterated, Organics www.PrepChem.com

Synthesis of benzyl p-toluenesulfonate

Synthesis of benzyl p-toluenesulfonate
Preparation of benzyl p-toluenesulfonate 22g of tosyl chloride were dissolved in 88 ml of dry ... Read more
Aug 22
1162 0 Esters, Organics, Organosulfur Compounds www.PrepChem.com

Synthesis of 4-chlorobutyl acetate

Synthesis of 4-chlorobutyl acetate
Preparation of 4-chlorobutyl acetate Acetyl chloride (65 g), tetrahydrofuran (50 g; b.p. 66°), ... Read more
Aug 21
980 0 Acetyl compounds, Halocarbons, Organics, Organochlorine Compounds www.PrepChem.com

Synthesis of 3-amino-2,4,6-triiodobenzoic acid

Synthesis of 3-amino-2,4,6-triiodobenzoic acid
Preparation of 3-amino-2,4,6-triiodobenzoic acid A mixture containing 290 g of iodine chloride ... Read more
Aug 21
697 0 Acids, Amines, Halocarbons, Organics, Organoiodine Compounds www.PrepChem.com
Synthesis submission

Synthesis of sodium dichloroiodate

Synthesis of sodium dichloroiodate
Preparation of sodium dichloroiodate Sodium dichloroiodate is prepared as 2M-soIution. 520g of ... Read more
Aug 21
1777 2 Chlorine Compounds, Inorganics, Iodine compounds, Sodium Compounds www.PrepChem.com

Synthesis of capronitrile

Synthesis of capronitrile
Preparation of capronitrile 30 g of dry sodium cyanide (dried at 110º C overnight a) are mixed ... Read more
Aug 21
728 0 Nitriles, Organics www.PrepChem.com

Synthesis of n-butane-1-d

Synthesis of n-butane-1-d
Preparation of n-butane-1-d 11 g of deuterium oxide are added slowly to a vigorously stirred ... Read more
Aug 21
891 0 Deuterated, Hydrocarbons, Organics www.PrepChem.com

Synthesis of picryl chloride

Synthesis of picryl chloride
Preparation of picryl chloride Pyridine (7.9) is added to a hot solution of picric acid (22.9 ... Read more
Aug 19
1464 0 Halocarbons, Nitro Compounds, Nitrocarbons, Organics, Organochlorine Compounds www.PrepChem.com

Synthesis of 4-chloro-1-butanol

Synthesis of 4-chloro-1-butanol
Preparation of 4-chloro-1-butanol 4-Chloro-1-butanol is obtained simply by leading hydrogen ... Read more
Aug 19
1481 0 Alcohols, Halocarbons, Organics, Organochlorine Compounds www.PrepChem.com
Synthesis submission
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The preparative procedures provided by PrepChem.com are intended for use ONLY by persons WITH PRIOR TRAINING in the field of CHEMISTRY. Although all syntheses are based on scientific literature with the citations to the original source, PrepChem.com does not warrant or guarantee the safety of individuals using these procedures. All synthesis procedures must be conducted at ONE’S OWN RISK. PrepChem.com disclaims any liability for any harm, loss, injuries, or damages claimed to have resulted from or related in any way to the procedures provided in PrepChem.com website.

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