Synthesis of 2-amino-2-thiazoline

Preparation of 2-amino-2-thiazoline 100 g of potassium thiocyanate are added to a solution of ... Read more

Synthesis of 3-chlorobenzaldehyde

Preparation of 3-chlorobenzaldehyde 2 moles of tin(II) chloride dihydrate are dissolved in ... Read more

Preparation of dichloromethyl methyl ether 832 g (4.0 moles) of phosphorus pentachloride and ... Read more

Preparation of 1,2-phenylene phosphorotrichloridite Chlorine is passed into a stirred ... Read more

Preparation of oxalyl bromide Oxalyl bromide is obtained by passing hydrogen bromide (8 ... Read more

Preparation of heptanenitrile 30 g of dry sodium cyanide (dried at 110º C overnight a) are ... Read more

Preparation of allyl alcohol-1,1-d2 6 g of lithium aluminum deuteride are made into a slurry ... Read more

Preparation of benzyl p-toluenesulfonate 22g of tosyl chloride were dissolved in 88 ml of dry ... Read more

Preparation of 4-chlorobutyl acetate Acetyl chloride (65 g), tetrahydrofuran (50 g; b.p. 66°), ... Read more

Preparation of 3-amino-2,4,6-triiodobenzoic acid A mixture containing 290 g of iodine chloride ... Read more

Preparation of sodium dichloroiodate Sodium dichloroiodate is prepared as 2M-soIution. 520g of ... Read more

Preparation of capronitrile 30 g of dry sodium cyanide (dried at 110º C overnight a) are mixed ... Read more

Preparation of n-butane-1-d 11 g of deuterium oxide are added slowly to a vigorously stirred ... Read more

Preparation of picryl chloride Pyridine (7.9) is added to a hot solution of picric acid (22.9 ... Read more

Preparation of 4-chloro-1-butanol 4-Chloro-1-butanol is obtained simply by leading hydrogen ... Read more