Synthesis of hydroxyacetone Preparation of hydroxyacetone Dowex 50 ion-exchange resin is treated with a solution of ... Read more
Synthesis of 6-hydroxy-6-methyl-2-heptanone Preparation of 6-hydroxy-6-methyl-2-heptanone A mixture of 6-methyl-5-hepten-2-one and 35% ... Read more
Synthesis of 1-phenyl-1,2-propanedione Preparation of 1-phenyl-1,2-propanedione 2N-Sulfuric acid (50 ml) containing mercury(II) ... Read more
Synthesis of 2-hexanone Preparation of 2-hexanone A mixture of 1 g of mercury(II) sulfate, 1 g of concentrated sulfuric ... Read more
Synthesis of 3-bromo-1,1-diphenylacetone Preparation of 3-bromo-1,1-diphenylacetone A solution of diphenylacetyl chloride (0.057 ... Read more
Synthesis of 4-phenyl-4-oxo-2-butenoic acid Preparation of 4-phenyl-4-oxo-2-butenoic acid (3-Benzoylacrylic acid) Aluminium trichloride was ... Read more
Synthesis of 1-(2,4-dihydroxyphenyl)-2-methoxyethan-1-one Preparation of 1-(2,4-dihydroxyphenyl)-2-methoxyethan-1-one 6.5 g of resorcinol are dissolved ... Read more
Synthesis of 1,1,3-tribromoacetone Preparation of 1,1,3-tribromoacetone 150 g of bromine dissolved in 500 ml of glacial acetic ... Read more
Synthesis of 4-hydroxy-4-methyl-2-pentanone Preparation of 4-hydroxy-4-methyl-2-pentanone 116 g of pure acetone are cooled to -12° C and ... Read more
Synthesis of 2-chlorocyclopentanone Preparation of 2-chlorocyclopentanone A rapid stream of gaseous chlorine is passed into a ... Read more
Synthesis of 1,3-dibromoacetone Preparation of 1,3-dibromoacetone 650 ml bromine (1.8 moles per 1 mole of acetone) are slowly ... Read more
Synthesis of camphorsulfonic acid Preparation of camphorsulfonic acid 45 g of camphor are finely powdered and added to a ... Read more
Synthesis of dehydroacetic acid Preparation of dehydroacetic acid 20 g of ethyl acetoacetate are boiled under a reflux for 6 ... Read more
Synthesis of 4-amino-3-methylbenzophenone Preparation of 4-amino-3-methylbenzophenone To a hot solution of 12.1 g. of ... Read more
Synthesis of 3′-aminoacetophenone Preparation of 3′-aminoacetophenone A solution of 295 g of 3-nitroacetophenone (Org. Syntheses ... Read more